Cy₃PAu-CC-(CH=CH)-CC-AuPCy₃

Base Information

• Chemical Name: Cy₃PAu-CC-(CH=CH)-CC-AuPCy₃
• CAS No.: 1231960-31-8
• Molecular Formula: C₄₂H₆₈Au₂P₂
• Molecular Weight: 1028.88
• Mol file: 1231960-31-8.mol

Synonyms:

Chemical Property of Cy₃PAu-CC-(CH=CH)-CC-AuPCy₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Cy₃PAu-CC-(CH=CH)-CC-AuPCy₃

There total 1 articles about Cy₃PAu-CC-(CH=CH)-CC-AuPCy₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(tricyclohexylphosphine)gold(I) chloride (49763-41-9) + (E)-1,6-hex-3-ene-1,5-diyne (92787-96-7) → Cy3PAu-CC-(CH=CH)-CC-AuPCy3 (1231960-31-8)

Guidance literature:

With sodium hydroxide; In methanol; (N2) to soln. Au complex and alkyne in MeOH NaOH was added and stirred for 1 h; ppt. was filtered, washed with water, MeOH and Et2O, column chromy. on alumina (CH2Cl2), product was dried in vacuo; elem. anal.;

DOI:10.1021/om1000919

upstream raw materials:

(tricyclohexylphosphine)gold(I) chloride

(E)-1,6-hex-3-ene-1,5-diyne