1-(trimethylstannyl)-3,3-pentamethylenepropadiene

Base Information

Chemical Name:1-(trimethylstannyl)-3,3-pentamethylenepropadiene
CAS No.:85366-26-3
Molecular Formula:C₁₁H₂₀Sn
Molecular Weight:270.99
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(trimethylstannyl)-3,3-pentamethylenepropadiene

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Technology Process of 1-(trimethylstannyl)-3,3-pentamethylenepropadiene

There total 1 articles about 1-(trimethylstannyl)-3,3-pentamethylenepropadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 85366-16-1
C₃H₉CuSn

: 59967-08-7
Methanesulfonic acid 1-ethynyl-cyclohexyl ester

: 85366-26-3
1-(trimethylstannyl)-3,3-pentamethylenepropadiene

Guidance literature:: In tetrahydrofuran; under N2, to stannylcopper(I) reagent added at -60°C propargyliccompd., stirred for 1 h at -60°C, poured into satd. soln. of NH4Cl in water contg. NaCN; extd. with ether/pentane, washed with water, dried with MgSO4, evapd. in vac., chromd. (Al2O3-5% H2O/n-hexane);
DOI:10.1016/S0022-328X(00)98533-4