trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3H2O0.25ethanol

Base Information

Chemical Name:trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol
CAS No.:72905-42-1
Molecular Formula:0C₂H₆O*C₁₄H₁₇CoN₅O₄*H₂O*NO₃
Molecular Weight:469.851
Hs Code.:

Synonyms:

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Chemical Property of trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol

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Technology Process of trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol

There total 2 articles about trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.5%

: cobalt(II) nitrate hexahydrate

: 37535-51-6,17407-39-5,37535-52-7
(S)-2-amino-3-(pyridin-2-yl)propanoic acid

: 71-00-1
L-histidine

: 28696-52-8
trans-carboxylate-(Co(L-histidinate)2)(1+)

: 18744-92-8
trans-imidazole-(Co(L-histidinate)2)(1+)

: 72982-76-4
trans-carboxylate-(Co(L-β-(2-pyridyl)-α-alaninate))(1+)

: 72905-42-1
trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol

: 72937-78-1
trans-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)](NO3)*2H2O

Guidance literature:: With sodium hydroxide; lead dioxide; In water; byproducts: trans-amino-Co(L-Pyala)2(1+); to a hot soln. contg. L-PyalaH, L-histidine and NaOH in water added Co(NO3)2*6H2O, soln. mixed for 15 min, PbO2 added, stirring and heating continued for 1 h; further products; soln. filtered, cooled to room temp., chromd., two bands crystd. from water, to which a layer of EtOH added, complexes contained both pyridine and imidazole unit; elem. anal. isomers of Co(L-His)2(1+) and Co(L-Pyala)2(1+) identified by NMR;
DOI:10.1021/ic50206a048

Reference yield:

: cobalt(II) nitrate hexahydrate

: 37535-51-6,17407-39-5,37535-52-7
(S)-2-amino-3-(pyridin-2-yl)propanoic acid

: 71-00-1
L-histidine

: 24419-71-4
trans-amino-(Co(L-histidinate)2)(1+)

: 72905-42-1
trans-carboxylate-[Co(L-β-(2-pyridyl)-α-alaninate)(L-histidinate)]NO3*H2O*0.25ethanol

Guidance literature:: With sodium hydroxide; lead dioxide; In water; to a hot soln. contg. L-PyalaH, L-histidine and NaOH in water added Co(NO3)2*6H2O, soln. mixed for 15 min, PbO2 added, stirring and heating continued for 1 h; further products; soln. filtered, cooled to room temp., chromd., two bands crystd. from water, to which a layer of EtOH added, complexes contained both pyridine and imidazole unit; elem. anal. isomers of Co(L-His)2(1+) and Co(L-Pyala)2(1+) identified by NMR;
DOI:10.1021/ic50206a048