Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid
CAS No.:143669-77-6
Molecular Formula:C₄₈H₅₃N₃O₁₃S
Molecular Weight:912.027
Hs Code.:

Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

There total 5 articles about Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55287-49-5
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 143669-77-6
Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / Ambient temperature

2: 98 percent / 0.1 N NaOMe / methanol; dioxane / 16 h / Ambient temperature; pH 8

3: 1.) 80percent NaH / 1.) THF, mineral oil, 15 min, 2.) r.t.

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 143669-73-2
2-O-Acetyl-3-O-allyl-4,6-O-benzyliden-α-D-glucopyranosyl-trichloracetimidat

: 143669-77-6
Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / Ambient temperature

2: 98 percent / 0.1 N NaOMe / methanol; dioxane / 16 h / Ambient temperature; pH 8

3: 1.) 80percent NaH / 1.) THF, mineral oil, 15 min, 2.) r.t.

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 143669-74-3
Benzyl-O-(2-O-acetyl-3-O-allyl-4,6-O-benzyliden-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

: 143669-77-6
Benzyl-O-(3-O-allyl-4,6-O-benzyliden-2-O-imidazolylsulfonyl-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 0.1 N NaOMe / methanol; dioxane / 16 h / Ambient temperature; pH 8

2: 1.) 80percent NaH / 1.) THF, mineral oil, 15 min, 2.) r.t.

With sodium methylate; sodium hydride; In 1,4-dioxane; methanol;