Technology Process of Benzenehexadecanoic acid, methyl ester
There total 17 articles about Benzenehexadecanoic acid, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
hexane;
at 20 ℃;
DOI:10.1021/jo061617n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / H2SO4 / Heating
2: 87 percent / Grubbs catalyst I / CH2Cl2 / Heating
3: 99 percent / H2 / Pd/C / hexane / 20 °C
With
sulfuric acid; hydrogen;
palladium on activated charcoal; Grubbs catalyst first generation;
In
hexane; dichloromethane;
2: olefin metathesis;
DOI:10.1021/jo061617n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / tetrahydrofuran / 2 h / 45 °C
1.2: 82 percent / CuCl / tetrahydrofuran / 1 h / 0 °C
2.1: 98 percent / H2SO4 / Heating
3.1: 87 percent / Grubbs catalyst I / CH2Cl2 / Heating
4.1: 99 percent / H2 / Pd/C / hexane / 20 °C
With
sulfuric acid; hydrogen; magnesium;
palladium on activated charcoal; Grubbs catalyst first generation;
In
tetrahydrofuran; hexane; dichloromethane;
3.1: olefin metathesis;
DOI:10.1021/jo061617n
