[Sc(p-tolyl)2(THF)4][BPh₄]

Base Information

• Chemical Name: [Sc(p-tolyl)2(THF)4][BPh₄]
• CAS No.: 960378-49-8
• Molecular Formula: C₂₄H₂₀B*C₃₀H₄₆O₄Sc
• Molecular Weight: 834.883

Synonyms:

Chemical Property of [Sc(p-tolyl)2(THF)4][BPh₄]

Chemical Property:

Purity/Quality:

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Technology Process of [Sc(p-tolyl)2(THF)4][BPh₄]

There total 2 articles about [Sc(p-tolyl)2(THF)4][BPh₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

[Sc(p-tolyl)3(THF)2] (960378-38-5) + triethylammonium tetraphenylborate → [Sc(p-tolyl)2(THF)4][BPh4] (960378-49-8)

Guidance literature:

In tetrahydrofuran; (Ar); soln. of (Et3NH)BPh4 (1 equiv.) in THF added dropwise at 0°C to soln. of Sc complex in THF; stirred at 0°C for 30 min; volatiles removed in vac.; washed with pentane; elem. anal.;

DOI:10.1021/om7007953

Reference yield:

[Sc(p-tolyl)3(THF)2] (960378-38-5) + triethylammonium tetraphenylborate → [Sc(p-tolyl)2(THF)4][BPh4] (960378-49-8) + [Sc(p-tolyl)(THF)5][BPh4]2

Guidance literature:

In tetrahydrofuran; (Ar); THF added to mixt. of Sc complex and (Et3NH)BPh4 (molar ratio 1:2)at -78°C; warmed slowly to room temp. overnight under stirring; supernatant decanted; ppt. washed with THF; volatiles removed under reduced pressure;

DOI:10.1021/om7007953

upstream raw materials:

[Sc(p-tolyl)3(THF)2]

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