(η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3]

Base Information

• Chemical Name: (η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3]
• CAS No.: 1310537-27-9
• Molecular Formula: C₃₂H₃₆Zn
• Molecular Weight: 486.028

Synonyms:

Chemical Property of (η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3]

Chemical Property:

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Technology Process of (η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3]

There total 1 articles about (η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

bis(pentamethylcyclopentadienyl)zinc + [2,6-(2,6-Me2C6H3)2C6H3]Li → (η5-C5Me5)Zn[2,6-(2,6-Me2C6H3)2C6H3] (1310537-27-9)

Guidance literature:

In diethyl ether; byproducts: LiCp*; (under Ar, Schlenk); ligand and Zn-complex mixed in Et2O, stirred for 20min at room temp.; filtered, solvent evapd. under reduced pressure, residue extd. with pentane, filtered, benzene added, put in fridge at -20°C, sepd., mother liquor transferred into flask, dried under vac.;

DOI:10.1021/ic200816f

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