dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV)

Base Information

Chemical Name:dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV)
CAS No.:1369393-98-5
Molecular Formula:C₃₃H₃₅F₁₂N₅Ti
Molecular Weight:777.535
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV)

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Technology Process of dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV)

There total 1 articles about dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: tetrakis(dimethylamido)titanium(IV)

: 1332334-12-9
1,1-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)-dipyrrol-5-ylmethane

: 1369393-98-5
dimethylaminebis(dimethylamido)(5,5-dimethyl-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)dipyrrolylmethane(-2H))titanium(IV)

Guidance literature:: In diethyl ether; under N2; ligand in Et2O and Ti compd. in Et2O frozen in liq. N2 separately; thawing soln. of ligand added to Ti compd.; warmed to room temp.; stirred overnight; volatiles removed under reduced pressure; oil triturated with pentane; crystd. from Et2O-pentane; elem. anal.;
DOI:10.1039/c1dt10127g