7-(4-tolyl)-5,12-diazabenzanthracen-6-ol

• Chemical Name: 7-(4-tolyl)-5,12-diazabenzanthracen-6-ol
• Molecular Formula: C₂₃H₁₆N₂O
• Molecular Weight: 336.393
• Mol file: 107263-30-9.mol

Synonyms:

Chemical Property of 7-(4-tolyl)-5,12-diazabenz

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-(4-tolyl)-5,12-diazabenz

There total 1 articles about 7-(4-tolyl)-5,12-diazabenzanthracen-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-anilino-quinolin-2-ol (6628-93-9) + p-Toluic acid (99-94-5) → 7-(4-tolyl)-5,12-diazabenzanthracen-6-ol (107263-30-9)

Guidance literature:

With zinc(II) chloride; at 285 ℃; for 3h;

Reference yield:

7-(4-tolyl)-5,12-diazabenzanthracen-6-ol (107263-30-9) → 6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene (107263-32-1)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; for 1.16667h; Heating;

Reference yield:

7-(4-tolyl)-5,12-diazabenzanthracen-6-ol (107263-30-9) → 6-anilino-7-(4-tolyl)-5,12-diazabenzanthracene (107263-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / dimethylformamide / 1.17 h / Heating

2: 71 percent / 0.83 h / Heating

With thionyl chloride; In N,N-dimethyl-formamide;

upstream raw materials:

4-anilino-quinolin-2-ol

p-Toluic acid

Downstream raw materials:

6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene

6-anilino-7-(4-tolyl)-5,12-diazabenzanthracene