Technology Process of C45H68N6O10Si2
There total 9 articles about C45H68N6O10Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 0 ℃;
for 6h;
DOI:10.1021/jo202159q
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 20 °C
2: iodoniumdicollidinium triflate / dichloromethane / 6 h / Inert atmosphere; Reflux
3: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 7 h / 70 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 6 h / 0 °C
With
copper(l) iodide; iodoniumdicollidinium triflate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo202159q
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iodoniumdicollidinium triflate / dichloromethane / 6 h / Inert atmosphere; Reflux
2: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 7 h / 70 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 6 h / 0 °C
With
copper(l) iodide; iodoniumdicollidinium triflate; caesium carbonate; trifluoroacetic acid; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202159q
