C₂₄H₃₃IO₁₃S

Base Information

Chemical Name:C₂₄H₃₃IO₁₃S
CAS No.:119803-66-6
Molecular Formula:C₂₄H₃₃IO₁₃S
Molecular Weight:688.489
Hs Code.:

C<sub>24</sub>H<sub>33</sub>IO<sub>13</sub>S

Synonyms:

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Chemical Property of C₂₄H₃₃IO₁₃S

Chemical Property:

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Technology Process of C₂₄H₃₃IO₁₃S

There total 10 articles about C₂₄H₃₃IO₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72718-62-8,81661-67-8,102281-77-6,120852-02-0,93417-43-7
1,2,3,6-tetra-O-acetyl-4-O-(2',3'-di-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranoside

: 119803-66-6
C₂₄H₃₃IO₁₃S

Guidance literature:: Multi-step reaction with 11 steps

1: 73 percent / triethylamine / CH₂Cl₂ / 24 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

3: 51 percent / sodium nitrite / dimethylformamide / 3 h / Ambient temperature

4: 97 percent / pyridine / CH₂Cl₂ / 0 deg C, , 30 min, RT, 3 h

5: tin tetrachloride / CHCl₃; nitromethane / 1.5 h / Ambient temperature

6: pyridine / methanol; CH₂Cl₂ / 24 h / Ambient temperature

7: pyridine / CH₂Cl₂

8: 44 percent / tetrahydrofuran / 24 h / Ambient temperature

9: 75 percent / 1,4-dithioerythritol, cysteamine / hexamethylphosphoric acid triamide / 0.67 h / Ambient temperature

10: 68 percent / ZnBr₂ / toluene / 2 h / 65 °C

11: 12 percent / 1M-sodium methoxide / methanol / Ambient temperature

With pyridine; 1,4-dithio-erythritol; sodium methylate; tin(IV) chloride; triethylamine; Cysteamine; zinc dibromide; sodium nitrite; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; nitromethane; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 119803-50-8
1,2,3,6-tetra-O-acetyl-4-O-(2,3-di-O-acetyl-6-O-benzoyl-α-D-glucopyranosyl)-β-D-glucopyranose

: 119803-66-6
C₂₄H₃₃IO₁₃S

Guidance literature:: Multi-step reaction with 10 steps

1: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 51 percent / sodium nitrite / dimethylformamide / 3 h / Ambient temperature

3: 97 percent / pyridine / CH₂Cl₂ / 0 deg C, , 30 min, RT, 3 h

4: tin tetrachloride / CHCl₃; nitromethane / 1.5 h / Ambient temperature

5: pyridine / methanol; CH₂Cl₂ / 24 h / Ambient temperature

6: pyridine / CH₂Cl₂

7: 44 percent / tetrahydrofuran / 24 h / Ambient temperature

8: 75 percent / 1,4-dithioerythritol, cysteamine / hexamethylphosphoric acid triamide / 0.67 h / Ambient temperature

9: 68 percent / ZnBr₂ / toluene / 2 h / 65 °C

10: 12 percent / 1M-sodium methoxide / methanol / Ambient temperature

With pyridine; 1,4-dithio-erythritol; sodium methylate; tin(IV) chloride; Cysteamine; zinc dibromide; sodium nitrite; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; nitromethane; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 119803-55-3,119803-75-7
Benzoic acid (2R,3S,4S,5R,6R)-4,5-diacetoxy-6-[(2R,3R,4S,5R)-4,5-diacetoxy-2-acetoxymethyl-6-(4-iodo-phenoxy)-tetrahydro-pyran-3-yloxy]-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

: 119803-66-6
C₂₄H₃₃IO₁₃S

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂

2: 44 percent / tetrahydrofuran / 24 h / Ambient temperature

3: 75 percent / 1,4-dithioerythritol, cysteamine / hexamethylphosphoric acid triamide / 0.67 h / Ambient temperature

4: 68 percent / ZnBr₂ / toluene / 2 h / 65 °C

5: 12 percent / 1M-sodium methoxide / methanol / Ambient temperature

With pyridine; 1,4-dithio-erythritol; sodium methylate; Cysteamine; zinc dibromide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;