p-BroMophenacyl Lactate

Base Information

• Chemical Name: p-BroMophenacyl Lactate
• CAS No.: 99853-28-8
• Molecular Formula: C₁₁H₁₁BrO₄
• Molecular Weight: 287.11
• Mol file: 99853-28-8.mol

Synonyms:

Chemical Property of p-BroMophenacyl Lactate

Chemical Property:

• Melting Point: 112-113 °C
• Boiling Point: 409.4±30.0 °C(Predicted)
• PKA: 12.79±0.20(Predicted)
• Density: 1.526±0.06 g/cm3(Predicted)

Purity/Quality:

p-BromophenacylLactate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: p-Bromophenacyl Lactate is a derivative of Lactic Acid, a compound produced from pyruvate via the enzyme lactate dehydrogenase in the process of fermentation during metabolism and exercise.

Technology Process of p-BroMophenacyl Lactate

There total 2 articles about p-BroMophenacyl Lactate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium salt of lactic acid (867-55-0) + para-bromophenacyl bromide (99-73-0,132309-76-3) → p-bromophenacyl rac-lactate (99853-28-8)

Guidance literature:

With potassium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

DOI:10.1021/acs.jnatprod.8b00101

Reference yield:

→ p-bromophenacyl rac-lactate (99853-28-8)

Guidance literature:

Na-Lactat, 4-Brom-phenacylbromid, Erwaermen;

DOI:10.1246/bcsj.33.1458

Reference yield:

p-bromophenacyl rac-lactate (99853-28-8) + trimethoxonium tetrafluoroborate (420-37-1) → p-bromophenacyl O-methyl-rac-lactate

Guidance literature:

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1021/acs.jnatprod.8b00101

upstream raw materials:

lithium salt of lactic acid

para-bromophenacyl bromide