5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

Base Information

Chemical Name:5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene
CAS No.:348-92-5
Molecular Formula:C₁₃H₇F₂I₂NO₄
Molecular Weight:533.009
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

Chemical Property:

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Technology Process of 5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

There total 9 articles about 5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 437-82-1
1,3-difluoro-2-methoxybenzene

: 348-92-5
5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: concentrated H₂SO₄; HNO₃

2: platinum; methanol / Hydrogenation

3: aqueous H₂SO₄; aqueous CuSO₄-solution; xylene / Diazotization

4: K₂CO₃; pentanone-⁽²⁾

With methanol; sulfuric acid; nitric acid; potassium carbonate; copper(II) sulfate; 2-Pentanone; platinum; xylene;
DOI:10.1021/ja01853a051

Reference yield:

: 392-25-6
1,3-difluoro-2-methoxy-5-nitrobenzene

: 348-92-5
5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: platinum; methanol / Hydrogenation

2: aqueous H₂SO₄; aqueous CuSO₄-solution; xylene / Diazotization

3: K₂CO₃; pentanone-⁽²⁾

With methanol; sulfuric acid; potassium carbonate; copper(II) sulfate; 2-Pentanone; platinum; xylene;
DOI:10.1021/ja01853a051

Reference yield:

: 319-60-8
3,5-difluoro-4-methoxybenzoic acid

: 348-92-5
5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride; diethyl ether; ammonia

2: aqueous alkaline sodium hypobromite

3: aqueous H₂SO₄; aqueous CuSO₄-solution; xylene / Diazotization

4: K₂CO₃; pentanone-⁽²⁾

With thionyl chloride; diethyl ether; alkaline sodium hypobromite; sulfuric acid; ammonia; potassium carbonate; copper(II) sulfate; 2-Pentanone; xylene;
DOI:10.1021/ja01853a051