4-Methyl-2-phthalimidopyridine

Base Information

• Chemical Name: 4-Methyl-2-phthalimidopyridine
• CAS No.: 106204-03-9
• Molecular Formula: C14H10N2O2
• Molecular Weight: 238.246
• DSSTox Substance ID: DTXSID20451338
• Wikidata: Q82271313
• ChEMBL ID: CHEMBL1875656

Synonyms:106204-03-9;2-(4-methylpyridin-2-yl)isoindoline-1,3-dione;4-methyl-2-phthalimidopyridine;MLS001199535;SCHEMBL501694;CHEMBL1875656;DTXSID20451338;DNJNBNSEZWBVOR-UHFFFAOYSA-N;HMS2883B08;SMR000560264;2-(4-methyl-pyridin-2-yl)-isoindole-1,3-dione;SR-01000127121;SR-01000127121-1;2-(4-methylpyridin-2-yl)-1H-isoindole-1,3(2H)-dione;2-(4-methylpyridin-2-yl)-2,3-dihydro-1H-isoindole-1,3-dione

Chemical Property of 4-Methyl-2-phthalimidopyridine

Chemical Property:

• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 238.074227566
• Heavy Atom Count: 18
• Complexity: 345

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=NC=C1)N2C(=O)C3=CC=CC=C3C2=O

Technology Process of 4-Methyl-2-phthalimidopyridine

There total 2 articles about 4-Methyl-2-phthalimidopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-Amino-4-methylpyridine (695-34-1) + phthalic anhydride (85-44-9) → 2-(4-methyl-2-pyridinyl)-1H-isoindole-1,3(2H)-dione (106204-03-9)

Guidance literature:

In acetic acid; for 24h; Heating;

DOI:10.1016/S0223-5234(01)01254-5

Reference yield:

phthalic anhydride (85-44-9) + 2-aminopicoline → 2-(4-methyl-2-pyridinyl)-1H-isoindole-1,3(2H)-dione (106204-03-9)

Guidance literature:

Reference yield: 23.0%

2-(4-methyl-2-pyridinyl)-1H-isoindole-1,3(2H)-dione (106204-03-9) → C14H9BrN2O2 (135995-35-6)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 20 - 80 ℃; Heating / reflux;

upstream raw materials:

2-Amino-4-methylpyridine

phthalic anhydride

Downstream raw materials:

C₁₄H₉BrN₂O₂

C₂₅H₃₁Cl₂N₅O₂

C₃₂H₃₀Cl₂N₄O₄

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