Technology Process of C27H38N2O2SSi
There total 16 articles about C27H38N2O2SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran
2: N-Bromosuccinimide / tetrahydrofuran
3: sodium diformamide / acetonitrile
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
5: 1H-imidazole / N,N-dimethyl-formamide
6: Lawessons reagent; pyridine / toluene / 100 °C
With
Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; sodium diformamide; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 8 steps
1: diisobutylaluminium hydride / toluene
3: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran
4: N-Bromosuccinimide / tetrahydrofuran
5: sodium diformamide / acetonitrile
6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
7: 1H-imidazole / N,N-dimethyl-formamide
8: Lawessons reagent; pyridine / toluene / 100 °C
With
Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; sodium diformamide; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067