dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide

Base Information

• Chemical Name: dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide
• CAS No.: 105996-39-2
• Molecular Formula: Br*C₂₁H₂₇BrNO₃
• Molecular Weight: 501.258
• Mol file: 105996-39-2.mol

Synonyms:

Chemical Property of dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide

There total 3 articles about dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

dl-1-(2,6-Dimethylphenoxy)-2-hydroxy-3-dimethylaminopropane (105996-35-8) + para-bromophenacyl bromide (99-73-0,132309-76-3) → dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide (105996-39-2)

Guidance literature:

In butanone; for 6h; Heating;

DOI:10.1007/BF00758612

Reference yield:

2.6-dimethylphenol (576-26-1,25134-01-4) → dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide (105996-39-2)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOH / H₂O

2: 74 percent / aq. ethanol / 10 h / 20 °C

3: 30 percent / butan-2-one / 6 h / Heating

With sodium hydroxide; In ethanol; water; butanone;

DOI:10.1007/BF00758612

Reference yield:

2,6-dimethylphenyl glycidyl ether (5296-34-4) → dl-N-<3-(2,6-Dimethylphenoxy)-2-hydroxypropyl>-N-(4-bromophenacyl)-N,N-dimethylammonium bromide (105996-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / aq. ethanol / 10 h / 20 °C

2: 30 percent / butan-2-one / 6 h / Heating

In ethanol; butanone;

DOI:10.1007/BF00758612

upstream raw materials:

dl-1-(2,6-Dimethylphenoxy)-2-hydroxy-3-dimethylaminopropane

para-bromophenacyl bromide

2,6-dimethylphenyl glycidyl ether

2.6-dimethylphenol

Refernces