C₄₆H₅₈N₈O₁₃S

Base Information

Chemical Name:C₄₆H₅₈N₈O₁₃S
CAS No.:1541175-35-2
Molecular Formula:C₄₆H₅₈N₈O₁₃S
Molecular Weight:963.078
Hs Code.:

C<sub>46</sub>H<sub>58</sub>N<sub>8</sub>O<sub>13</sub>S

Synonyms:

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Chemical Property of C₄₆H₅₈N₈O₁₃S

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Technology Process of C₄₆H₅₈N₈O₁₃S

There total 14 articles about C₄₆H₅₈N₈O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541175-34-1
4-((2S)-3-methoxy-3-oxo-2-((2S,4R)-4-(4-((3-oxo-1-phenyl-2,8,11,14-tetraoxa-4-azaheptadecan-17-yl)carbamoyl)-1H-1,2,3-triazol-1-yl)-1-(phenylsulfonyl)pyrrolidine-2-carboxamido)propyl)phenyl pyrrolidine-1-carboxylate

: 1541175-35-2
C₄₆H₅₈N₈O₁₃S

Guidance literature:: 4-((2S)-3-methoxy-3-oxo-2-((2S,4R)-4-(4-((3-oxo-1-phenyl-2,8,11,14-tetraoxa-4-azaheptadecan-17-yl)carbamoyl)-1H-1,2,3-triazol-1-yl)-1-(phenylsulfonyl)pyrrolidine-2-carboxamido)propyl)phenyl pyrrolidine-1-carboxylate; With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; ethanol; water;
DOI:10.1039/c3ob42332h

Reference yield:

: 13512-31-7
N-(benzyloxycarbonyl)-L-tyrosine methyl ester

: 1541175-35-2
C₄₆H₅₈N₈O₁₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 0.75 h / 100 °C / Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

3.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: sodium L-ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 60 °C

5.1: sodium hydroxide / water; tetrahydrofuran; ethanol / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3ob42332h

Reference yield:

: 1192-63-8
1-pyrrolidinecarbonyl chloride

: 1541175-35-2
C₄₆H₅₈N₈O₁₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 0.75 h / 100 °C / Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

3.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: sodium L-ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 60 °C

5.1: sodium hydroxide / water; tetrahydrofuran; ethanol / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3ob42332h