ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

Base Information

Chemical Name:ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate
CAS No.:126245-89-4
Molecular Formula:C₁₉H₂₈FNO₂
Molecular Weight:321.435
Hs Code.:

Synonyms:

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Chemical Property of ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

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Technology Process of ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

There total 4 articles about ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126245-80-5
ethyl 8-methyl-7-oxononanoate

: 126245-89-4
ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / N-bromosuccinimide / CCl₄ / 5 h / Heating

2: 55 percent / lithium bromide / dimethylformamide / 1 h / 95 °C

3: 75 percent / hydroxylammonium chloride / ethanol / 5 h / Heating

4: 1.) zinc powder, acetic acid / 1.) room temperature, 2.) room temperature, 2 h

With N-Bromosuccinimide; hydroxylamine hydrochloride; acetic acid; lithium bromide; zinc; In tetrachloromethane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 126245-82-7
ethyl 8-methyl-7-oxo-8-nonenoate

: 126245-89-4
ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydroxylammonium chloride / ethanol / 5 h / Heating

2: 1.) zinc powder, acetic acid / 1.) room temperature, 2.) room temperature, 2 h

With hydroxylamine hydrochloride; acetic acid; zinc; In ethanol;

Reference yield:

: 126245-81-6
ethyl 8-bromo-8-methyl-7-oxononanoate

: 126245-89-4
ethyl 7-(4-fluorobenzylidenimino)-8-methylnonanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / lithium bromide / dimethylformamide / 1 h / 95 °C

2: 75 percent / hydroxylammonium chloride / ethanol / 5 h / Heating

3: 1.) zinc powder, acetic acid / 1.) room temperature, 2.) room temperature, 2 h

With hydroxylamine hydrochloride; acetic acid; lithium bromide; zinc; In ethanol; N,N-dimethyl-formamide;