Technology Process of C30H32N2O3Si
There total 4 articles about C30H32N2O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C36H39N3O4Si;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 0.833333h;
Inert atmosphere;
With
oxygen; ethyl acetate;
In
tetrahydrofuran; diethyl ether;
at 0 - 20 ℃;
for 1.5h;
Air atmosphere;
DOI:10.1021/jo202286a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
2.2: 0.25 h / -78 °C / Inert atmosphere
2.3: -78 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.83 h / 0 °C / Inert atmosphere
3.2: 1.5 h / 0 - 20 °C / Air atmosphere
With
lithium aluminium tetrahydride; n-butyllithium; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo202286a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
1.2: 0.25 h / -78 °C / Inert atmosphere
1.3: -78 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.83 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 0 - 20 °C / Air atmosphere
With
lithium aluminium tetrahydride; n-butyllithium;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo202286a
