C₃₂H₂₅NO₅S

Base Information

Chemical Name:C₃₂H₂₅NO₅S
CAS No.:137648-54-5
Molecular Formula:C₃₂H₂₅NO₅S
Molecular Weight:535.62
Hs Code.:

C<sub>32</sub>H<sub>25</sub>NO<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₂₅NO₅S

Chemical Property:

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Technology Process of C₃₂H₂₅NO₅S

There total 11 articles about C₃₂H₂₅NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 137648-53-4,141395-20-2
C₃₂H₂₅NO₃S

: 137648-54-5,141395-21-3
C₃₂H₂₅NO₅S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/ja00026a039

Reference yield:

: 130012-94-1
N-<(phenyloxy)carbonyl>-6a,10a-epoxy-6-ethynyl-10-oxo-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 137648-54-5,141395-21-3
C₃₂H₂₅NO₅S

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / Et₃N, Pd(Ph₃)4, cuprous iodide / benzene / 2 h / 40 °C

2: 84 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 0.67 h / 25 °C

3: 89 percent / lithium diisopropylamide / toluene; cyclohexane / 0.17 h / -78 °C

4: 81 percent / 4-(dimethylamino)pyridine (DMAP) / CH₂Cl₂ / 168 h / 25 °C

5: 94 percent / n-Bu₃SnH, azoisobutyronitrile (AIBN) / toluene / 1 h / 25 °C

6: 1.) NaH / 1.) THF, 25 deg C, 5 min, 2.) THF, 25 deg C, 10 min

7: 81 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 0.5 h / 25 °C

With dmap; lithium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; cyclohexane; water; toluene; benzene;
DOI:10.1021/ja00071a003

Reference yield:

: 137648-50-1,141395-15-5
C₃₀H₂₁NO₄

: 137648-54-5,141395-21-3
C₃₂H₂₅NO₅S

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / 4-(dimethylamino)pyridine (DMAP) / CH₂Cl₂ / 168 h / 25 °C

2: 94 percent / n-Bu₃SnH, azoisobutyronitrile (AIBN) / toluene / 1 h / 25 °C

3: 1.) NaH / 1.) THF, 25 deg C, 5 min, 2.) THF, 25 deg C, 10 min

4: 81 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 0.5 h / 25 °C

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/ja00071a003