C₂₅H₃₅O₃P

Base Information

Chemical Name:C₂₅H₃₅O₃P
CAS No.:2351219-90-2
Molecular Formula:C₂₅H₃₅O₃P
Molecular Weight:414.525
Hs Code.:

C<sub>25</sub>H<sub>35</sub>O<sub>3</sub>P

Synonyms:

Suppliers and Price of C₂₅H₃₅O₃P

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of C₂₅H₃₅O₃P

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₃₅O₃P

There total 6 articles about C₂₅H₃₅O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₂₅H₃₅O₄P

: 2351219-90-2,2444702-33-2,2634687-68-4
C₂₅H₃₅O₃P

Guidance literature:: With titanium(IV) isopropylate; In tetrahydrofuran; at 70 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00194

Reference yield:

: 1338453-90-9
(S)-3-(tert-butyl)-4-hydroxy-2H-benzo[d][1,3]oxaphosphole 3-oxide

: 2351219-90-2,2444702-33-2,2634687-68-4
C₂₅H₃₅O₃P

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 10 h / 100 °C / Inert atmosphere; Schlenk technique

3: N-Bromosuccinimide / acetonitrile / 20 °C / Inert atmosphere; Schlenk technique

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere; Schlenk technique

5: palladium(II) hydroxide; hydrogen / tetrahydrofuran / 16 h / 20 °C

6: titanium(IV) isopropylate / tetrahydrofuran / 70 °C / Inert atmosphere; Schlenk technique

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; titanium(IV) isopropylate; potassium fluoride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; hydrogen; palladium(II) hydroxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;
DOI:10.1021/acs.organomet.9b00194

Reference yield:

: 1338453-95-4
(S)-3-tert-butyl-2,3-dihydrobenzo[d][1,3]oxaphosphol-4-yl trifluoromethanesulfonate oxide

: 2351219-90-2,2444702-33-2,2634687-68-4
C₂₅H₃₅O₃P

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 10 h / 100 °C / Inert atmosphere; Schlenk technique

2: N-Bromosuccinimide / acetonitrile / 20 °C / Inert atmosphere; Schlenk technique

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere; Schlenk technique

4: palladium(II) hydroxide; hydrogen / tetrahydrofuran / 16 h / 20 °C

5: titanium(IV) isopropylate / tetrahydrofuran / 70 °C / Inert atmosphere; Schlenk technique

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; titanium(IV) isopropylate; potassium fluoride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; hydrogen; palladium(II) hydroxide; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile;
DOI:10.1021/acs.organomet.9b00194