N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat

Base Information

• Chemical Name: N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat
• CAS No.: 75085-67-5
• Molecular Formula: C₈₁H₈₇Cl₂N₁₁O₁₆P₂Si₂
• Molecular Weight: 1659.67

Synonyms:

Chemical Property of N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat

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Useful:

Technology Process of N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat

There total 2 articles about N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(o-chlorphenyl)(β-cyanethyl)phosphat (75074-02-1) + C49H50ClN5O9PSi(1-) → N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N6-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat (75085-67-5)

Guidance literature:

With triisipropylbenzenesulfonyl nitrotriazolide; Yield given;

DOI:10.1016/S0040-4039(00)93649-9

Reference yield:

N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(o-chlorphenyl)(β-cyanethyl)phosphat (75074-02-1) + Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenosin-2'-(2-chlorphenyl)phosphat> (75082-94-9) → N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N6-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat (75085-67-5)

Guidance literature:

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; Yield given. Multistep reaction; 1) pyridine; 2) pyridine, 16 h at room temp.;

Reference yield: 90.0%

N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N6-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat (75085-67-5) + triethylamine (121-44-8) → Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat> (80727-22-6)

Guidance literature:

In pyridine; for 2.5h; Ambient temperature;

upstream raw materials:

N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(o-chlorphenyl)(β-cyanethyl)phosphat

Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenosin-2'-(2-chlorphenyl)phosphat>

Downstream raw materials:

C₇₈H₈₄Cl₂N₁₀O₁₆P₂Si₂

Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>

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