(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

Base Information

Chemical Name:(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid
CAS No.:78089-20-0
Molecular Formula:C₂HF₃O₂*C₂₆H₂₂N₂O₆
Molecular Weight:572.494
Hs Code.:

(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

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Chemical Property of (S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

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Technology Process of (S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

There total 3 articles about (S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 78089-18-6
(S)-2-Benzyloxycarbonylamino-3-tert-butoxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester

: 76-05-1
trifluoroacetic acid

: 78089-20-0
(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

Guidance literature:: In water; for 3.5h; Ambient temperature;
DOI:10.1021/jo00331a001

Reference yield:

: 7598-10-9
2-(bromomethyl)anthraquinone

: 78089-20-0
(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / 0.5 h / Heating

2: 87 percent / H₂O / 3.5 h / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water;
DOI:10.1021/jo00331a001

Reference yield:

: 16947-84-5,62234-36-0
N-[(benzyloxy)carbonyl]-3-[(tert-butoxycarbonyl)amino]-L-alanine

: 78089-20-0
(S)-3-Amino-2-benzyloxycarbonylamino-propionic acid 9,10-dioxo-9,10-dihydro-anthracen-2-ylmethyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / 0.5 h / Heating

2: 87 percent / H₂O / 3.5 h / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water;
DOI:10.1021/jo00331a001