(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

Base Information

Chemical Name:(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate
CAS No.:1432584-85-4
Molecular Formula:C₃₇H₄₅N₅O₉
Molecular Weight:703.792
Hs Code.:

(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

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Chemical Property of (10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

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Technology Process of (10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

There total 8 articles about (10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1432584-84-3
(S,Z)-N-((S)-2-(((benzyloxy)carbonyl)amino)-5-(1,3-bis((benzyloxy)carbonyl)guanidino)pentylidene)-1-(tertbutoxy)-1-oxopropan-2-amine oxide

: 1432584-85-4
(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

: 84765-39-9
(S)-tert-butyl 2-formamidopropanoate

Guidance literature:: In benzene; at 40 ℃; for 1.5h; Inert atmosphere; UV-irradiation;
DOI:10.1002/anie.201300504

Reference yield:

: 14611-34-8
N^α,N^δ,N^ω-tris(benzyloxycarbonyl)-L-arginine

: 1432584-85-4
(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.1: dichloromethane / 20 °C / Inert atmosphere

4.1: benzene / 1.5 h / 40 °C / Inert atmosphere; UV-irradiation

With lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1002/anie.201300504

Reference yield:

: 151012-20-3
C₃₂H₃₇N₅O₈

: 1432584-85-4
(10S,13S)-tert-butyl 6-((benzyloxy)carbonyl)-10-(((benzyloxy)carbonyl)amino)-5-imino-13-methyl-3,11-dioxo-1-phenyl-2-oxa-4,6,12-triazatetradecan-14-oate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2: dichloromethane / 20 °C / Inert atmosphere

3: benzene / 1.5 h / 40 °C / Inert atmosphere; UV-irradiation

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1002/anie.201300504