Technology Process of C17H18N2OS
There total 5 articles about C17H18N2OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonia;
In
methanol;
at 60 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetraphosphorus decasulfide; pyridine / 1 h / 120 °C / Inert atmosphere
2: ammonia / methanol / 16 h / 60 °C / Inert atmosphere
With
pyridine; tetraphosphorus decasulfide; ammonia;
In
methanol;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis(triphenylphosphine)palladium(II)-chloride; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / 80 °C / Inert atmosphere
2: ammonia / methanol / 3 h / 150 °C / Microwave irradiation; Inert atmosphere
3: tetraphosphorus decasulfide; pyridine / 1 h / 120 °C / Inert atmosphere
4: ammonia / methanol / 16 h / 60 °C / Inert atmosphere
With
pyridine; bis(triphenylphosphine)palladium(II)-chloride; tetraphosphorus decasulfide; ammonia; sodium carbonate;
In
methanol; 1,2-dimethoxyethane; water;
DOI:10.1021/jm3011349