Technology Process of C30H21F3N2O7
There total 9 articles about C30H21F3N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus tribromide / dichloromethane / 10 - 25 °C
2: potassium tert-butylate / N,N-dimethyl-formamide / 10 - 25 °C
3: water; potassium hydroxide / methanol / 25 °C
With
potassium tert-butylate; water; phosphorus tribromide; potassium hydroxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.08.031
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / dimethyl sulfoxide / 0 - 25 °C
2: sodium tetrahydroborate / methanol / 10 - 25 °C
3: phosphorus tribromide / dichloromethane / 10 - 25 °C
4: potassium tert-butylate / N,N-dimethyl-formamide / 10 - 25 °C
5: water; potassium hydroxide / methanol / 25 °C
With
sodium tetrahydroborate; potassium tert-butylate; water; phosphorus tribromide; sodium hydride; potassium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.08.031