(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

Base Information

Chemical Name:(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan
CAS No.:97909-52-9
Molecular Formula:C₃₂H₃₂OP₂
Molecular Weight:494.553
Hs Code.:

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Chemical Property of (+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

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Technology Process of (+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

There total 2 articles about (+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 97909-53-0,97949-72-9,97949-73-0,133814-14-9
(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan-P,P'-dioxid

: 97909-52-9,97949-74-1
(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

Guidance literature:: With trichlorosilane;

Reference yield: 63.0%

: 97909-51-8
(2-endo,3-exo)-7-oxabicyclo<2.2.1>heptane-2,3-dimethanol bis(4-methylbenzenesulfonate)

: 4376-01-6
sodium diphenylphosphide

: 97909-52-9,97949-74-1
(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

Guidance literature:: In tetrahydrofuran; 1,4-dioxane;

Reference yield: 90.0%

: nickel(II) chloride hexahydrate

: 97909-52-9,97949-74-1
(+)-trans-2,3-Bis(diphenylphosphinomethyl)-7-oxanorbornan

: (C₆H₅)2PCH₂C₆H₈OCH₂P(C₆H₅)2NiCl₂

Guidance literature:: In ethanol; to soln. of NiCl2*6H2O in EtOH added hot soln. of C6H8O(CH2PPh2)2, react. time 5-7 h under Ar; filtered, washed with EtOH, dried in vac., elem.anal.;
DOI:10.1016/0022-328X(87)85186-0