Technology Process of C39H53FO5
There total 6 articles about C39H53FO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
dodecyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside;
With
triethylsilane; trifluoroacetic acid;
In
dichloromethane;
With
pyridine; trifluoromethylsulfonic anhydride;
In
dichloromethane;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
Further stages.;
DOI:10.1016/j.jfluchem.2007.02.013
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 100 percent / NaOMe; MeOH
2.1: CSA / dimethylformamide
3.1: NaH / dimethylformamide
4.1: Et3SiH; TFA / CH2Cl2
4.2: Tf2O; pyridine / CH2Cl2
4.3: tetrabutylammonium fluoride / tetrahydrofuran
With
methanol; triethylsilane; camphor-10-sulfonic acid; sodium methylate; sodium hydride; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2007.02.013
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 51 percent / BF3*Et2O / 1,2-dichloro-ethane
2.1: 100 percent / NaOMe; MeOH
3.1: CSA / dimethylformamide
4.1: NaH / dimethylformamide
5.1: Et3SiH; TFA / CH2Cl2
5.2: Tf2O; pyridine / CH2Cl2
5.3: tetrabutylammonium fluoride / tetrahydrofuran
With
methanol; triethylsilane; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; trifluoroacetic acid;
In
dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2007.02.013
