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Technology Process of {RuCl3(CH3(C6H5)2As)3}

{RuCl3(CH3(C6H5)2As)3}

Base Information
  • Chemical Name:{RuCl3(CH3(C6H5)2As)3}
  • CAS No.:55147-41-6
  • Molecular Formula:C39H39As3Cl3Ru
  • Molecular Weight:939.932
  • Hs Code.:
{RuCl<sub>3</sub>(CH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2As)3}

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Chemical Property of {RuCl3(CH3(C6H5)2As)3}
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Technology Process of {RuCl3(CH3(C6H5)2As)3}

There total 1 articles about {RuCl3(CH3(C6H5)2As)3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium aquapentachlororuthenate(III)

potassium aquapentachlororuthenate(III)

diphenylmethylarsine
945-48-2

diphenylmethylarsine

{RuCl<sub>3</sub>(CH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2As)3}
55147-41-6,66673-37-8

{RuCl3(CH3(C6H5)2As)3}

Guidance literature:
With ethanol; In ethanol; reduction of 10 ml K2(RuCl5H2O) soln. contg. 0.1 g Ru on boiling with 40 ml ethanol, addn. of 0.7 g methyldiphenylarsine in 20 ml ethanol; boiling the soln. for 10 min; cooling, shaking with petroleum ether;;

Reference yield:

{RuCl<sub>3</sub>(C<sub>13</sub>H<sub>13</sub>As)3}
66673-37-8,55147-41-6

{RuCl3(C13H13As)3}

trans-{RuCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>3</sub>)4}

trans-{RuCl2((C6H5)2AsCH3)4}

Guidance literature:
With HPH2O2; In ethanol; heating the Ru compound with 30% HPH2O2 in sufficient alcohol under reflux, until the soln. has turned light yellow;; pptn. by water in presence of petroleum ether;;
upstream raw materials:

diphenylmethylarsine

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