2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

Base Information

Chemical Name:2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester
CAS No.:126257-56-5
Molecular Formula:C₂₈H₃₈O₆
Molecular Weight:470.606
Hs Code.:

2,6-Anhydro-5-O-<4'-<trans-4''-(n-heptyl)cyclohexyl>benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

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Chemical Property of 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

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Technology Process of 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

There total 4 articles about 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 81930-19-0
trans-4-(4-Heptylcyclohexyl)benzoesaeurechlorid

: 126257-51-0
2,6-Anhydro-3,4,7-tridesoxy-L-ribo-hept-3-enonsaeuremethylester

: 126257-56-5
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

: 126257-54-3,126373-55-5
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enonsaeure-methylester

Guidance literature:: With pyridine; for 1h;

Reference yield:

: 34819-86-8
3,4-di-O-acetyl-6-deoxy-L-glucal

: 126257-56-5
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Et₂O*BF₃ / acetonitrile / 0.17 h

2: 1) AcCl 2) conc. HCl / 1) r.t.

3: 3 percent / pyridine / 1 h

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; acetyl chloride; In acetonitrile;

Reference yield:

: 93978-97-3
4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl cyanide

: 126257-56-5
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-erythro-hept-2-en-4-ulonsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) AcCl 2) conc. HCl / 1) r.t.

2: 3 percent / pyridine / 1 h

With pyridine; hydrogenchloride; acetyl chloride;