9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol

Base Information

Chemical Name:9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol
CAS No.:23526-81-0
Molecular Formula:C₁₁H₁₁BrO
Molecular Weight:239.112
Hs Code.:
NSC Number:122950
DSSTox Substance ID:DTXSID50946282

Synonyms:23526-81-0;9-bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol;NSC122950;DTXSID50946282;NSC-122950

Suppliers and Price of 9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol

Chemical Property:

Vapor Pressure:2.23E-05mmHg at 25°C
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:237.99933
Heavy Atom Count:13
Complexity:218

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2C(C(C1O)C3=CC=CC=C23)Br

Technology Process of 9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol

There total 6 articles about 9-Bromo-1,2,3,4-tetrahydro-1,4-methanonaphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4453-90-1
1,4-dihydro-1,4-methanonaphthalene

: 23526-81-0
syn-7-Brom-exo-2-hydroxy-benzonorbornen

Guidance literature:: Multi-step reaction with 2 steps

1: (i) 1,2-dibromo-1,1,2,2-tetrachloro-ethane, (irradiation), (ii) /BRN= 506007/, Ag₂O, Ac₂O

2: MeMgI

With methyl magnesium iodide;
DOI:10.1021/jo00830a065

Reference yield:

: syn-7-Brom-exo-2-acetoxy-benzonorbornen

: 23526-81-0
syn-7-Brom-exo-2-hydroxy-benzonorbornen

Guidance literature:: With methyl magnesium iodide;
DOI:10.1021/ja01028a046 DOI:10.1021/jo00830a065

Reference yield:

: 2,3-trans-Dibromobenzonorborn-5-ene

: 23526-81-0
syn-7-Brom-exo-2-hydroxy-benzonorbornen

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH

2: MeMgI

With methyl magnesium iodide; acetic acid;
DOI:10.1021/ja01028a046