tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

Base Information

Chemical Name:tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron
CAS No.:132080-67-2
Molecular Formula:C₁₉H₁₂FeO₅S
Molecular Weight:408.214
Hs Code.:

Synonyms:

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Chemical Property of tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

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Technology Process of tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

There total 2 articles about tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 15321-51-4
diiron nonacarbonyl

: 54119-53-8
3,4-diphenylthiopnene 1,1-dioxide

: 132080-67-2
tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

Guidance literature:: In tetrahydrofuran; byproducts: Fe3(CO)12; under inert gas; a solution of 3,4-DPTDO was treated with Fe2(CO)9; stirred for 5 h under exclusion of light; evaporated to dryness; chromd.; elution with petroleum ether/toluene; than with ethyl acetate; elem. anal.;
DOI:10.1016/0022-328X(90)80095-H

Reference yield: 44.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 54119-53-8
3,4-diphenylthiopnene 1,1-dioxide

: 132080-67-2
tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

Guidance literature:: In dichloromethane; Irradiation (UV/VIS); under inert gas; a solution of 3,4-DPTDO was treated with Fe(CO)5; mixt. irradiated for 7 h; filtration; evaporated to dryness; chromy.; elution with toluene, toluene/ ethyl acetate (5:1), ethyl acetate; evaporation; pentane was added; elem. anal.;
DOI:10.1016/0022-328X(90)80095-H

Reference yield: 25.0%

: 132080-67-2
tricarbonyl(η4-3,4-diphenylthiophene dioxide)iron

: 132080-90-1
Fe(CO)2(P(C₆H₅)3)(C₄H₂(C₆H₅)2SO₂)

Guidance literature:: With PPh₃; In toluene; under inert gas; a solution of the Fe-complex and PPh3 was irradiated for 6 h; evaporated to dryness; residue extracted with pentane; residue treated with ethyl acetate/ hexane (1:1); chromy.; elem. anal.;
DOI:10.1016/0022-328X(90)80095-H