dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum

Base Information

• Chemical Name: dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum
• CAS No.: 130461-36-8
• Molecular Formula: C₂₄H₂₁Cl₂MoNO₄P₂
• Molecular Weight: 616.229

Synonyms:

Chemical Property of dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum

Chemical Property:

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Technology Process of dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum

There total 1 articles about dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[MoCl3(NP(C6H5)2NP(C6H5)2N)] + triphenylhydroxysilane (791-31-1) → dichloro(1,3-dioxo-1,1,3,3-tetraphenyldi-λ5-phosphazane-O,O')dioxo-molybdenum (130461-36-8)

Guidance literature:

In tetrahydrofuran; acetic anhydride; byproducts: hexaphenyldisiloxane; under dry N2 atm., Ph3SiOH in THF is added to stirred soln. of molybdaphosphazene in acetic anhydride at room temp. (2 d); filtn. (Celite), concn. of solvent volume; elem. anal.;

DOI:10.1039/DT9900002387

upstream raw materials:

triphenylhydroxysilane

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