C₁₇H₂₄O₆S

Base Information

Chemical Name:C₁₇H₂₄O₆S
CAS No.:1328886-35-6
Molecular Formula:C₁₇H₂₄O₆S
Molecular Weight:356.44
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>6</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₄O₆S

Chemical Property:

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Technology Process of C₁₇H₂₄O₆S

There total 8 articles about C₁₇H₂₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1328886-34-5
C₁₀H₁₈O₄

: 98-59-9
p-toluenesulfonyl chloride

: 1328886-35-6
C₁₇H₂₄O₆S

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1055/s-0030-1260586

Reference yield:

: 1328886-22-1
C₂₂H₂₉NO₇

: 1328886-35-6
C₁₇H₂₄O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / tetrahydrofuran; methanol / 1 h / Reflux

2.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 1 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium tert-butylate / tetrahydrofuran; toluene / 1.5 h / 20 °C

4.2: 20 °C

5.1: ammonia; sodium / tetrahydrofuran / 4 h / -78 °C

6.1: pyridine / 0 - 20 °C

With pyridine; lithium borohydride; oxalyl dichloride; potassium tert-butylate; ammonia; sodium; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1055/s-0030-1260586

Reference yield:

: 1328886-21-0
C₁₉H₂₅NO₅

: 1328886-35-6
C₁₇H₂₄O₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

1.2: -78 - -45 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Inert atmosphere; Reflux

3.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / tetrahydrofuran; methanol / 1 h / Reflux

4.1: lithium borohydride / tetrahydrofuran; methanol; diethyl ether / 1 h / 0 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C

5.2: -78 - 0 °C

6.1: potassium tert-butylate / tetrahydrofuran; toluene / 1.5 h / 20 °C

6.2: 20 °C

7.1: ammonia; sodium / tetrahydrofuran / 4 h / -78 °C

8.1: pyridine / 0 - 20 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; oxalyl dichloride; potassium tert-butylate; ammonia; sodium hexamethyldisilazane; sodium; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1055/s-0030-1260586