C₁₇H₂₇NO₉S₃

Base Information

• Chemical Name: C₁₇H₂₇NO₉S₃
• CAS No.: 1314079-82-7
• Molecular Formula: C₁₇H₂₇NO₉S₃
• Molecular Weight: 485.601
• Mol file: 1314079-82-7.mol

Synonyms:

Chemical Property of C₁₇H₂₇NO₉S₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₇NO₉S₃

There total 12 articles about C₁₇H₂₇NO₉S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H21NO5S (1123693-96-8) → C17H27NO9S3 (1314079-82-7)

Guidance literature:

Multi-step reaction with 8 steps

1: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

2: methanol; sodium hydroxide / water / 1 h

3: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

4: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

5: methanol; sodium hydroxide / water / 1 h

6: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

7: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

8: formic acid; dihydrogen peroxide / 2 h / 20 °C

With methanol; formic acid; dihydrogen peroxide; caesium carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.084

Reference yield:

benzyl 4-mercapto-2-methylbutan-2-ylcarbamate (1226913-81-0) → C17H27NO9S3 (1314079-82-7)

Guidance literature:

Multi-step reaction with 6 steps

1: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

2: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

3: methanol; sodium hydroxide / water / 1 h

4: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

5: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

6: formic acid; dihydrogen peroxide / 2 h / 20 °C

With methanol; formic acid; dihydrogen peroxide; caesium carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.084

Reference yield:

C19H29NO3S3 → C17H27NO9S3 (1314079-82-7)

Guidance literature:

With formic acid; dihydrogen peroxide; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2011.04.084

upstream raw materials:

C₁₄H₂₁NO₅S

benzyl 4-mercapto-2-methylbutan-2-ylcarbamate

3-Methylbutenoic acid

1-hydroxy-3-methylbut-3-ylamine