[Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄]

Base Information

Chemical Name:[Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄]
CAS No.:1313228-52-2
Molecular Formula:C₂₄H₂₀B*C₃₁H₂₈N₅NiS₂
Molecular Weight:912.653
Hs Code.:

[Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh<sub>4</sub>]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄]

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Technology Process of [Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄]

There total 1 articles about [Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 66-71-7
1,10-Phenanthroline

: nickel(II) chloride hexahydrate

: [Ni(hexamethyleneimine dithiocarbamate)2]

: 143-66-8
sodium tetraphenyl borate

: 1313228-52-2
[Ni(hexamethyleneimine dithiocarbamate)(1,10-phenanthroline)2][BPh₄]

Guidance literature:: In ethanol; EtOH suspn. of Ni compd. mixed with EtOH soln. of ligand, mixt. stirred for 10 min, NiCl2*6H2O and NaBPh4 added (1:4:1:2 molar ratio), mixt. refluxed for 10 h; hot soln. filtered, crystd. on cooling, filtered off, washed (H2O, EtOH,Et2O), dried (40°C), elem. anal.;
DOI:10.1016/j.ica.2011.03.010