N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-9-<2'-O-<(tert-butyl)d...

Base Information

• Chemical Name: N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-9-<2'-O-<(tert-butyl)d...
• CAS No.: 132849-93-5
• Molecular Formula: C₁₀₅H₁₂₀FN₁₇O₂₃P₂Si₃
• Molecular Weight: 2153.41
• Mol file: 132849-93-5.mol

Synonyms:

Chemical Property of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-9-<2'-O-<(tert-butyl)d...

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-9-<2'-O-<(tert-butyl)d...

There total 1 articles about N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-9-<2'-O-<(tert-butyl)d... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N6-Benzoyl-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-fluoro-β-D-xylofuranosyl>adenine (132849-71-9) + N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-<2-(4-nitrophenyl)ethyl triethylammonium phosphate> (128060-12-8) → N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N6-benzoyl-9-<2'-O-<(tert-butyl)d... (132849-93-5)

Guidance literature:

With 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; In pyridine; Ambient temperature;

DOI:10.1002/hlca.19910740104

Reference yield:

N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N6-benzoyl-9-<2'-O-<(tert-butyl)d... (132849-93-5) → C89H106FN15O19P2Si3

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine; for 24h; Ambient temperature;

DOI:10.1002/hlca.19910740104

upstream raw materials:

N⁶-Benzoyl-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-fluoro-β-D-xylofuranosyl>adenine

N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-<2-(4-nitrophenyl)ethyl>>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-<2-(4-nitrophenyl)ethyl triethylammonium phosphate>