(3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate

Base Information

• Chemical Name: (3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate
• CAS No.: 1145688-70-5
• Molecular Formula: C₂₂H₂₄N₂S₂
• Molecular Weight: 380.578
• Mol file: 1145688-70-5.mol

Synonyms:

Chemical Property of (3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate

There total 1 articles about (3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

carbon disulfide (75-15-0,12122-00-8) + (1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine (65838-10-0,135613-88-6,143443-23-6,191480-61-2) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → (3R,7R)-1,3-dibenzyl-3,4,5,6,7,7-hexahydrobenzoimidazol-1-ium-2-dithiocarboxylate (1145688-70-5)

Guidance literature:

(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine; N,N-dimethyl-formamide dimethyl acetal; at 100 ℃; for 48h; Inert atmosphere;

carbon disulfide; In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 0.75h; Inert atmosphere;

DOI:10.1055/s-0028-1083317

upstream raw materials:

carbon disulfide

(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine

N,N-dimethyl-formamide dimethyl acetal