Technology Process of C15H16O
There total 4 articles about C15H16O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver trifluoromethanesulfonate;
In
dichloromethane;
at 22 ℃;
regioselective reaction;
Inert atmosphere;
DOI:10.1002/chem.201102476
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0 - 45 °C
1.2: 20 - 45 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0 - 45 °C
2.2: 20 - 45 °C
3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
4.1: silver trifluoromethanesulfonate / dichloromethane / 22 °C / Inert atmosphere
With
oxalyl dichloride; silver trifluoromethanesulfonate; N,N-dimethyl-formamide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
4.1: Kondakov-Darzens olefin acylation;
DOI:10.1002/chem.201102476
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
2: silver trifluoromethanesulfonate / dichloromethane / 22 °C / Inert atmosphere
With
oxalyl dichloride; silver trifluoromethanesulfonate; N,N-dimethyl-formamide;
In
dichloromethane;
2: Kondakov-Darzens olefin acylation;
DOI:10.1002/chem.201102476
