1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane

Base Information

• Chemical Name: 1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane
• CAS No.: 149575-22-4
• Molecular Formula: C₂₉H₄₂B₂N₂
• Molecular Weight: 440.288
• Mol file: 149575-22-4.mol

Synonyms:

Chemical Property of 1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane

There total 1 articles about 1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

6,8-bis(diisopropylamino)-3,3-bis(η5-cyclopentadienyl)-2,4-diphenyl-6,8-dibora-3-zirconabicyclo{3.3.0}octa-1,4-diene → 1,3-bis(diisopropylamino)-4,5-bis-(cis-phenylmethylidene)-1,3-diborolane (149575-22-4)

Guidance literature:

With HCl; In diethyl ether; (under N2); addn. of a soln. of HCl in diethyl ether to the starting complex in diethyl ether at -40°C, stirring for 14 h; removal of the solvent in vac., rsidue ia suspd. in hexane, filtn. from Cp2ZrCl2, concg. of the filtrate, recrystn. of the ppt. at -78°C, elem. anal.;

DOI:10.1021/om00031a009