(π-tetravinylsilane)bis(triphenylphosphine)dinickel

Base Information

Chemical Name:(π-tetravinylsilane)bis(triphenylphosphine)dinickel
CAS No.:86811-75-8
Molecular Formula:C₄₄H₄₂Ni₂P₂Si
Molecular Weight:778.231
Hs Code.:

Synonyms:

Suppliers and Price of (π-tetravinylsilane)bis(triphenylphosphine)dinickel

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (π-tetravinylsilane)bis(triphenylphosphine)dinickel

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (π-tetravinylsilane)bis(triphenylphosphine)dinickel

There total 3 articles about (π-tetravinylsilane)bis(triphenylphosphine)dinickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 1112-55-6
tetravinylsilane

: 603-35-0
triphenylphosphine

: 86811-75-8
(π-tetravinylsilane)bis(triphenylphosphine)dinickel

Guidance literature:: In benzene; stirred for 24 h at room temp.; volatiles removed (vac.), moved into pentane, filtered (Celite), concd.,pptd. at -30°C for 2 d; elem. anal.;
DOI:10.1016/j.jorganchem.2004.06.057

Reference yield: 81.0%

: 23777-40-4
bis(triphenylphosphine)ethylenenickel⁽⁰⁾

: 1112-55-6
tetravinylsilane

: 86811-75-8
(π-tetravinylsilane)bis(triphenylphosphine)dinickel

Guidance literature:: In not given;
DOI:10.1016/j.jorganchem.2004.06.057

Reference yield:

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 1112-55-6
tetravinylsilane

: 86811-75-8
(π-tetravinylsilane)bis(triphenylphosphine)dinickel

: 86811-74-7
(π-tetravinylsilane)triphenylphosphinenickel

Guidance literature:: With triphenylphosphine; In benzene; (Ar); PPh3 (1 equiv) soln. added to complex and tetravinylsilane mixt. in C6H6 at 22°C, stirred for 18 h; evapd., dissolved in ether, treated with pentane, ppt. filtered off, washed with pentane, dried (vac.); obtained as mixt.;
DOI:10.1016/S0022-328X(00)98719-9