tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V)

Base Information

Chemical Name:tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V)
CAS No.:74185-18-5
Molecular Formula:C₅N₅OS₅Tc*2C₂₄H₂₀As
Molecular Weight:1171.01
Hs Code.:

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Chemical Property of tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V)

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Technology Process of tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V)

There total 1 articles about tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: ammonium thiocyanate

: {n-Bu₄N}TcOCl₄

: 104170-16-3
tetraphenylarsonium chloride monohydrate

: 74185-18-5
tetraphenylarsonium oxopentakis(isothiocyanato)technetate(V)

Guidance literature:: In methanol; soln. of Tc-compd. in MeOH cooled to 0°C on ice bath, 4.9 equiv of NH4SCN added, after 1 min Ph4AsCl*H2O added; solid collected, washed with MeOH, dried in vac.; elem. anal.;
DOI:10.1021/ic50218a040