GeI₂(1,2-bis(diphenylphosphino)benzene)

Base Information

• Chemical Name: GeI₂(1,2-bis(diphenylphosphino)benzene)
• CAS No.: 1204668-47-2
• Molecular Formula: C₃₀H₂₄GeI₂P₂
• Molecular Weight: 772.867

Synonyms:

Chemical Property of GeI₂(1,2-bis(diphenylphosphino)benzene)

Chemical Property:

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Technology Process of GeI₂(1,2-bis(diphenylphosphino)benzene)

There total 1 articles about GeI₂(1,2-bis(diphenylphosphino)benzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

o-phenylenebis(diphenylphosphine) (13991-08-7) + germanium(II) iodide → GeI2(1,2-bis(diphenylphosphino)benzene) (1204668-47-2)

Guidance literature:

In acetonitrile; under N2; diphosphine added to soln. of Ge compd. in CH3CN at room temp., mixt. stirred for 30 min; evapn. under vac., residue washed with Et2O, dried under vac., recrystn.from CH3CN by slow evapn.; elem. anal.;

DOI:10.1021/ic902068z

upstream raw materials:

o-phenylenebis(diphenylphosphine)

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