C₂₃H₁₂F₆N₂O₄

Base Information

Chemical Name:C₂₃H₁₂F₆N₂O₄
CAS No.:1276038-43-7
Molecular Formula:C₂₃H₁₂F₆N₂O₄
Molecular Weight:494.35
Hs Code.:

C<sub>23</sub>H<sub>12</sub>F<sub>6</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₃H₁₂F₆N₂O₄

Chemical Property:

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Technology Process of C₂₃H₁₂F₆N₂O₄

There total 8 articles about C₂₃H₁₂F₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276040-71-1
C₂₃H₁₄F₆N₂O₄

: 1276038-43-7
C₂₃H₁₂F₆N₂O₄

Guidance literature:: With iodine; sodium carbonate; In deuteromethanol; at 20 ℃; for 3h;
DOI:10.1021/jm4004522

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1276038-43-7
C₂₃H₁₂F₆N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sodium cyanoborohydride; acetic acid / 16 h / 0 - 20 °C

2: 2-methoxy-ethanol / 4 h / Reflux

3: sodium tetrahydroborate / methanol / 16 h / 20 °C

4: caesium carbonate / N,N-dimethyl-formamide / 24 h / 50 °C

5: sodium hydroxide / methanol; tetrahydrofuran / 96 h / 20 °C

6: iodine; sodium carbonate / deuteromethanol / 3 h / 20 °C

With sodium tetrahydroborate; iodine; sodium cyanoborohydride; sodium carbonate; caesium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; deuteromethanol; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm4004522

Reference yield:

: 1276040-03-9
C₁₄H₁₀F₃NO₃

: 1276038-43-7
C₂₃H₁₂F₆N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 2-methoxy-ethanol / 4 h / Reflux

2: sodium tetrahydroborate / methanol / 16 h / 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 24 h / 50 °C

4: sodium hydroxide / methanol; tetrahydrofuran / 96 h / 20 °C

5: iodine; sodium carbonate / deuteromethanol / 3 h / 20 °C

With sodium tetrahydroborate; iodine; sodium carbonate; caesium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; deuteromethanol; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm4004522