α-fluoro-p-coumaric acid

Base Information

Chemical Name:α-fluoro-p-coumaric acid
CAS No.:18238-96-5
Molecular Formula:C₉H₇FO₃
Molecular Weight:182.151
Hs Code.:

Synonyms:

Suppliers and Price of α-fluoro-p-coumaric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-fluoro-p-coumaric acid

Chemical Property:

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Technology Process of α-fluoro-p-coumaric acid

There total 6 articles about α-fluoro-p-coumaric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930106-43-7
C₁₁H₁₁FO₃

: 18238-96-5
α-fluoro-p-coumaric acid

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 3h;
DOI:10.1562/2006-01-17-RA-781

Reference yield:

: 930106-40-4
C₁₇H₂₅FO₃Si

: 18238-96-5
α-fluoro-p-coumaric acid

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₄NF / H₂O; tetrahydrofuran / 3 h / 20 °C

2: KOH / methanol / 3 h / 20 °C

With potassium hydroxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; water;
DOI:10.1562/2006-01-17-RA-781

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 18238-96-5
α-fluoro-p-coumaric acid

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / benzene / 2 h / Heating

2: Bu₄NF / H₂O; tetrahydrofuran / 3 h / 20 °C

3: KOH / methanol / 3 h / 20 °C

With potassium hydroxide; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; methanol; water; benzene; 1: Horner reaction;
DOI:10.1562/2006-01-17-RA-781