C₂₈H₂₂N₂O₂

Base Information

Chemical Name:C₂₈H₂₂N₂O₂
CAS No.:1395922-96-9
Molecular Formula:C₂₈H₂₂N₂O₂
Molecular Weight:418.495
Hs Code.:

C<sub>28</sub>H<sub>22</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₂₈H₂₂N₂O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₈H₂₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₈H₂₂N₂O₂

There total 6 articles about C₂₈H₂₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 3973-54-4
2-chloro-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one

: 16091-26-2
N-Benzoyl-m-phenylendiamin

: 1395922-96-9
C₂₈H₂₂N₂O₂

Guidance literature:: With palladium diacetate; caesium carbonate; XPhos; In toluene; tert-butyl alcohol; at 90 ℃; Inert atmosphere;
DOI:10.1021/jm300951u

Reference yield:

: 119-67-5
o-carboxybenzaldehyde

: 1395922-96-9
C₂₈H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine / methanol / 2 h / Reflux

1.2: 3.75 h / 0 °C

2.1: 10% Pd/C; hydrogen / ethyl acetate; acetonitrile / 5 h / 20 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: aluminum (III) chloride / dichloromethane / 4 h / 20 °C

5.1: caesium carbonate; palladium diacetate; XPhos / tert-butyl alcohol; toluene / 90 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; 10% Pd/C; hydrogen; palladium diacetate; caesium carbonate; N,N-dimethyl-formamide; triphenylphosphine; XPhos; In methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination / 4.1: |Friedel-Crafts Acylation / 5.1: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u

Reference yield:

: C₁₅H₁₂Cl₂O

: 1395922-96-9
C₂₈H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 4 h / 20 °C

2: caesium carbonate; palladium diacetate; XPhos / tert-butyl alcohol; toluene / 90 °C / Inert atmosphere

With aluminum (III) chloride; palladium diacetate; caesium carbonate; XPhos; In dichloromethane; toluene; tert-butyl alcohol; 1: |Friedel-Crafts Acylation / 2: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u