Clopidogrel IMpurity 2 (Clopidogrel IMiniuM IMpurity)

Base Information

• Chemical Name: Clopidogrel IMpurity 2 (Clopidogrel IMiniuM IMpurity)
• CAS No.: 1396607-49-0
• Molecular Formula: Br*C₁₆H₁₅ClNO₂S
• Molecular Weight: 400.724
• Mol file: 1396607-49-0.mol

Synonyms:

Chemical Property of Clopidogrel IMpurity 2 (Clopidogrel IMiniuM IMpurity)

Chemical Property:

• Melting Point: 166 - 169°C
• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

95+% ^*data from raw suppliers

5-[(1S)-1-(2-Chlorophenyl)-2-methoxy-2-oxoethyl]-6,7-dihydro-Thieno[3,2-c]pyridiniumBromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 5-[(1S)-1-(2-Chlorophenyl)-2-methoxy-2-oxoethyl]-6,7-dihydro-Thieno[3,2-c]pyridinium bromide (1:1), is an impurity of Clopidogrel (C587250), an antithrombotic.

Technology Process of Clopidogrel IMpurity 2 (Clopidogrel IMiniuM IMpurity)

There total 1 articles about Clopidogrel IMpurity 2 (Clopidogrel IMiniuM IMpurity) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(±)-clopidogrel hydrochloride → 5-[(2-chlorophenyl)(methoxycarbonyl)methyl]-6,7-dihydrothieno[3,2-c]pyridin-5-ium bromide (1396607-49-0)

Guidance literature:

(±)-clopidogrel hydrochloride; With N-Bromosuccinimide; In dichloromethane; at 0 - 5 ℃; for 8.25h;

In dichloromethane; at 20 ℃; for 36h;

DOI:10.1021/op300110m

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