C₂₂H₃₆S

Base Information

Chemical Name:C₂₂H₃₆S
CAS No.:1393672-13-3
Molecular Formula:C₂₂H₃₆S
Molecular Weight:332.594
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₆S

Chemical Property:

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Technology Process of C₂₂H₃₆S

There total 3 articles about C₂₂H₃₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-53-8
phenylmethanethiol

: 3,3-dihexylcycloprop-1-ene

: 1393672-13-3
C₂₂H₃₆S

Guidance literature:: With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I); In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/jo300930c

Reference yield:

: 19780-80-4
6-methylenetridecane

: 1393672-13-3
C₂₂H₃₆S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / dichloromethane / 35 °C

2: ethylmagnesium bromide; titanium(IV) isopropylate / tetrahydrofuran / 4.5 h / 20 °C

3: potassium tert-butylate / dimethyl sulfoxide / 55 °C

4: [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I) / dichloromethane / 0.5 h / 25 °C

With titanium(IV) isopropylate; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I); ethylmagnesium bromide; potassium tert-butylate; sodium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jo300930c

Reference yield:

: 1393672-10-0
1,1-dibromo-2,2-dihexylcyclopropane

: 1393672-13-3
C₂₂H₃₆S

Guidance literature:: Multi-step reaction with 3 steps

1: ethylmagnesium bromide; titanium(IV) isopropylate / tetrahydrofuran / 4.5 h / 20 °C

2: potassium tert-butylate / dimethyl sulfoxide / 55 °C

3: [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I) / dichloromethane / 0.5 h / 25 °C

With titanium(IV) isopropylate; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I); ethylmagnesium bromide; potassium tert-butylate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jo300930c