1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

Base Information

Chemical Name:1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene
CAS No.:235103-11-4
Molecular Formula:C₂₈H₃₄N₂O
Molecular Weight:414.591
Hs Code.:

Synonyms:

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Chemical Property of 1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

Chemical Property:

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Technology Process of 1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

There total 5 articles about 1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 235103-10-3
1-(2-phenyl-2-oxoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

: 235103-11-4
1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

Guidance literature:: With potassium hydroxide; magnesium sulfate; mercury(II) oxide; In ethanol; pentane;
DOI:10.1021/jo990172i

Reference yield:

: 92373-44-9
dicyclohexylacetic acid chloride

: 235103-11-4
1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: AlCl₃ / 1 h

2.1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / 24 h / Heating

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -40 °C

3.2: tetrahydrofuran; hexane / 2 h / -40 °C

4.1: 63 percent / HgCl₂; HgO / methanol; H₂O / 5 h / Heating

5.1: MgSO₄; HgO; KOH / pentane; ethanol

With potassium hydroxide; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; magnesium sulfate; mercury dichloride; mercury(II) oxide; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; hexane; water; pentane; 1.1: Acylation / 2.1: Bromination / 3.1: Metallation / 3.2: Substitution / 4.1: Hydrolysis / 5.1: Dehydrogenation;
DOI:10.1021/jo990172i

Reference yield:

: 52034-92-1
dicyclohexylacetic acid

: 235103-11-4
1-(2-phenyl-2-diazoethyl)-4-(2,2-dicyclohexyl-1-oxoethyl)benzene

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / CH₂Cl₂ / 1.5 h / Heating

2.1: AlCl₃ / 1 h

3.1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / 24 h / Heating

4.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -40 °C

4.2: tetrahydrofuran; hexane / 2 h / -40 °C

5.1: 63 percent / HgCl₂; HgO / methanol; H₂O / 5 h / Heating

6.1: MgSO₄; HgO; KOH / pentane; ethanol

With potassium hydroxide; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; thionyl chloride; magnesium sulfate; mercury dichloride; mercury(II) oxide; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; hexane; dichloromethane; water; pentane; 1.1: Chlorination / 2.1: Acylation / 3.1: Bromination / 4.1: Metallation / 4.2: Substitution / 5.1: Hydrolysis / 6.1: Dehydrogenation;
DOI:10.1021/jo990172i