2H-Pyran-3-ol, 3-[[(4,5-dihydro-1H-imidazol-2-yl)amino]methyl]tetrahydro-2-(4-methoxy phenyl)-2-methyl-

Base Information

Chemical Name:2H-Pyran-3-ol, 3-[[(4,5-dihydro-1H-imidazol-2-yl)amino]methyl]tetrahydro-2-(4-methoxy phenyl)-2-methyl-
CAS No.:106281-39-4
Molecular Formula:C₁₇H₂₅N₃O₃
Molecular Weight:319.404
Hs Code.:

Synonyms:

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Chemical Property of 2H-Pyran-3-ol, 3-[[(4,5-dihydro-1H-imidazol-2-yl)amino]methyl]tetrahydro-2-(4-methoxy phenyl)-2-methyl-

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-Pyran-3-ol, 3-[[(4,5-dihydro-1H-imidazol-2-yl)amino]methyl]tetrahydro-2-(4-methoxy phenyl)-2-methyl-

There total 7 articles about 2H-Pyran-3-ol, 3-[[(4,5-dihydro-1H-imidazol-2-yl)amino]methyl]tetrahydro-2-(4-methoxy phenyl)-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106281-25-8
6-hydroxy-2-(p-methoxyphenyl)-2-methyl-2H-pyran-3(6H)-one

: 106281-39-4
tetrahydro-3-(1-imidazolin-2-ylamino)methyl-2-(p-methoxyphenyl)-2-methyl-2H-pyran-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / Et₃N / CH₂Cl₂ / 1) 5-10 deg C, 0.5 h, r.t., 20 min, 2) r.t, 3 h,

2: H₂ / 10percent Pd/C / ethyl acetate / 3.5 h / 760 Torr / Ambient temperature

3: 90 percent / NH₄Cl / aq. ethanol / 10 h

4: H₂ / platinum oxide / acetic acid; HCl / 6 h / 2585.7 Torr

5: butan-1-ol / 1) reflux, 5 h, 2) r.t., overnight

With hydrogen; ammonium chloride; triethylamine; platinum(IV) oxide; palladium on activated charcoal; In hydrogenchloride; ethanol; dichloromethane; acetic acid; ethyl acetate; butan-1-ol;

Reference yield:

: 106281-24-7
α-p-methoxyphenyl-α-methylfurfuryl alcohol

: 106281-39-4
tetrahydro-3-(1-imidazolin-2-ylamino)methyl-2-(p-methoxyphenyl)-2-methyl-2H-pyran-3-ol

Guidance literature:: Multi-step reaction with 6 steps

1: m-chloroperbenzoic acid / CH₂Cl₂ / 2.5 h

2: 87 percent / Et₃N / CH₂Cl₂ / 1) 5-10 deg C, 0.5 h, r.t., 20 min, 2) r.t, 3 h,

3: H₂ / 10percent Pd/C / ethyl acetate / 3.5 h / 760 Torr / Ambient temperature

4: 90 percent / NH₄Cl / aq. ethanol / 10 h

5: H₂ / platinum oxide / acetic acid; HCl / 6 h / 2585.7 Torr

6: butan-1-ol / 1) reflux, 5 h, 2) r.t., overnight

With hydrogen; ammonium chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; platinum(IV) oxide; palladium on activated charcoal; In hydrogenchloride; ethanol; dichloromethane; acetic acid; ethyl acetate; butan-1-ol;

Reference yield:

: 106281-30-5
5,6-dihydro-2-(p-methoxyphenyl)-2-methyl-2H-pyran-3(4H)-one

: 106281-39-4
tetrahydro-3-(1-imidazolin-2-ylamino)methyl-2-(p-methoxyphenyl)-2-methyl-2H-pyran-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NH₄Cl / aq. ethanol / 10 h

2: H₂ / platinum oxide / acetic acid; HCl / 6 h / 2585.7 Torr

3: butan-1-ol / 1) reflux, 5 h, 2) r.t., overnight

With hydrogen; ammonium chloride; platinum(IV) oxide; In hydrogenchloride; ethanol; acetic acid; butan-1-ol;